Instrumentation
Lab 13.02 phone 53826, 52634
Spectrometer AVANCE700
700 MHz Protonenresonanz
Manufacturerersteller: BRUKER BIOSPIN
Built in 2008
Equipped with a BRUKER Triple resonance (1H, 13C, 15N, 2D) cryoprobe (1H and 13C coil at 17K). Magnet: Bruker Ultra shield plus. Raw data can be downloaded in BRUKER TOPSPIN format (recommended) www.chemie.fu-berlin.de/nmrdata/700AV/nmr (../delta JEOL Delta format).
In addition this lab houses the
Spectrometer ECZ600 S
600 MHz proton- resonance
Manufacturer: JEOL
Build in 2018
Solid state NMR. 3.2 mm MAS probe. Low gamma nuclei. Raw data can be downloaded from www.chemie.fu-berlin.de/nmrdata/600S/delta (JEOL Delta format)
Office 13.01 phone 53826
Office and computer workplace >
The spectrometer AV700 is run from this office. Additionally there are two computer workplaces (one of which is used by members of Christian Freund' s group).
Lab 13.14 phone 56286
Spectrometer ECZ600
600 MHz proton- resonance
Manufacturer: JEOL
Built in 2018
Cryo probe operating at nitrogen temperature. Nuclei 1H 19F 13C 31P 29Si 15N. 24 slot sample changer. Raw data can be downloaded www.chemie.fu-berlin.de/nmrdata/600ECZ/delta (nmr). Replacement for spectrometer AC250
.
Lab 13.12 phone 52630
Spectrometer ECP500
500 MHz proton- resonance
Manufacturer: JEOL
Built in 2000
The spectrometer is equipped with an inverse probe together with a GRASP unit. It can be operated manually, if special experiments are requested, or by use of a sample changer for all sort of routine measuerements. Raw data can be accessed via www.chemie.fu-berlin.de/nmrdata/500ECP/delta (nmr).
Lab 13.07 phone 55670
Spectrometer AVANCE500
500 MHz proton- resonance
Manufacturer: BRUKER BIOSPIN
Built in 2008
Equipped with two field gradient units to perform GRASP experiments and DOSY measurement, BRUKER BCUX to allow for measurements down to -60 C, sample changer and several probes including an ultra low temperature probe, a DOSY probe
and an 10 mm broadband probehead.
Raw data are accessible BRUKER TOPSPIN format (recommended) via
www.chemie.fu-berlin.de/nmrdata/500AV/nmr (../delta JEOL Delta format).
Lab 13.15 phone 52767
Spektrometer ECX400
400 MHz proton- resonance
Manufacturer: JEOL
Built in 2005
Equipped with an automatically tuneable probe (nuclei 13C, 31P, 11B, 2D and 19F). Mainly sampler changer operation. Outside of service hours the spectrometer is open to working group members (assigned to this task by their group leader). Raw data can be found at www.chemie.fu-berlin.de/nmrdata/400ECX/delta (nmr).
SupraFAB Building
Spectrometer ECZ400
400 MHz proton- resonance
Manufacturer: JEOL
Built in 2021
400 MHz proton resonnace Equipped with HR-MAS probe and field gradient unit to be used for semi solid samples Raw data are transferred to www.chemie.fu-berlin.de/nmrdata/4003sHR/delta (../delta JEOL Delta format).
Lab 14.12 phone 55516
Spectrometer DPX 400
400 MHz proton- resonance
Manufacturer: BRUKER BIOSPIN
Built in 1996 out of order
Hand operated. The spectrometer has been shifted to Takustr. 3 by the end of 2010 and has been upgradet with HR MAS equipment. Raw data are transferred to www.chemie.fu-berlin.de/nmrdata/400DPX/nmr (../delta JEOL Delta format).