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Elementaranalyse

Takustraße 3
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Instrumentation

Lab 13.02 phone 53826, 52634

Spectrometer AVANCE700 AVIII 700

700 MHz Protonenresonanz

Manufacturerersteller: BRUKER BIOSPIN

Built in 2008

Equipped with a BRUKER Triple resonance (1H, 13C, 15N, 2D) cryoprobe (1H and 13C coil at 17K). Magnet: Bruker Ultra shield plus. Raw data can be downloaded in BRUKER TOPSPIN format (recommended) www.chemie.fu-berlin.de/nmrdata/700AV/nmr (../delta JEOL Delta format).

In addition this lab houses the

Spectrometer ECZ600 S Solid State NMR

600 MHz proton- resonance

Manufacturer: JEOL

Build in 2018

Solid state NMR. 3.2 mm MAS probe. Low gamma nuclei. Raw data can be downloaded from www.chemie.fu-berlin.de/nmrdata/600S/delta (JEOL Delta format)

Office 13.01 phone 53826

Office and computer workplace Buero

The spectrometer AV700 is run from this office. Additionally there are two computer workplaces (one of which is used by members of Christian Freund' s group).

Lab 13.14 phone 56286

Spectrometer ECZ600 AC250

600 MHz proton- resonance

Manufacturer: JEOL

Built in 2018

Cryo probe operating at nitrogen temperature. Nuclei 1H 19F 13C 31P 29Si 15N. 24 slot sample changer. Raw data can be downloaded www.chemie.fu-berlin.de/nmrdata/600ECZ/delta (nmr). Replacement for spectrometer AC250 AV500

.

Lab 13.12 phone 52630

Spectrometer ECP500 ECP500

500 MHz proton- resonance

Manufacturer: JEOL

Built in 2000

The spectrometer is equipped with an inverse probe together with a GRASP unit. It can be operated manually, if special experiments are requested, or by use of a sample changer for all sort of routine measuerements. Raw data can be accessed via www.chemie.fu-berlin.de/nmrdata/500ECP/delta (nmr).

Lab 13.07 phone 55670

Spectrometer AVANCE500 AVIII 500

500 MHz proton- resonance

Manufacturer: BRUKER BIOSPIN

Built in 2008

Equipped with two field gradient units to perform GRASP experiments and DOSY measurement, BRUKER BCUX to allow for measurements down to -60 C, sample changer and several probes including an ultra low temperature probe, a DOSY probe

AV500

and an 10 mm broadband probehead.

Raw data are accessible BRUKER TOPSPIN format (recommended) via www.chemie.fu-berlin.de/nmrdata/500AV/nmr (../delta JEOL Delta format).

Lab 13.15 phone 52767

Spektrometer ECX400 ECX400

400 MHz proton- resonance

Manufacturer: JEOL

Built in 2005

Equipped with an automatically tuneable probe (nuclei 13C, 31P, 11B, 2D and 19F). Mainly sampler changer operation. Outside of service hours the spectrometer is open to working group members (assigned to this task by their group leader). Raw data can be found at www.chemie.fu-berlin.de/nmrdata/400ECX/delta (nmr).

SupraFAB Building

Spectrometer ECZ400 ECZ 400

400 MHz proton- resonance

Manufacturer: JEOL

Built in 2021

400 MHz proton resonnace Equipped with HR-MAS probe and field gradient unit to be used for semi solid samples Raw data are transferred to www.chemie.fu-berlin.de/nmrdata/4003sHR/delta (../delta JEOL Delta format).

Lab 14.12 phone 55516

Spectrometer DPX 400 DPX 400

400 MHz proton- resonance

Manufacturer: BRUKER BIOSPIN

Built in 1996 out of order

Hand operated. The spectrometer has been shifted to Takustr. 3 by the end of 2010 and has been upgradet with HR MAS equipment. Raw data are transferred to www.chemie.fu-berlin.de/nmrdata/400DPX/nmr (../delta JEOL Delta format).

 

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