CRYOPROTECTIN, A CABBAGE PROTEIN PROTECTING THYLAKOIDS FROM
FREEZE-THAW DAMAGE

Silke Schilling (1), Hany A. M. Sror (2), Dirk K. Hincha (3), Jürgen M. Schmitt (1), Carsten A. Köhn (1)

(1) Institut für Pflanzenphysiologie und Mikrobiologie, Freie Universität, Königin-Luise-Str. 12-16, 14195
Berlin, Germany
(2) Permanent address: Biochemistry Department, Faculty of Agriculture, Ain-shams University, Cairo,
Egypt
(3) Present address: Max-Planck Institut für Molekulare Pflanzenphysiologie, 14424 Potsdam, Germany

We have purified a protein (cryoprotectin) from the leaves of cold-acclimated savoy cabbage (Brassica
oleracea L. convar. capitata (L.) Alef. var. sabauda L.), which protects thylakoids isolated from the leaves of
non-acclimated spinach (Spinacia oleracea) from freeze-thaw damage. Sequencing of cryoprotectin revealed
the copurification of at least three isoforms. The sequence data showed homology to the WAX9 protein
family, which belongs to the class of nonspecific lipid transfer proteins (Hincha et al., Plant Physiology, Vol.
125, pp. 835-846). Antibodies raised against a synthetic peptide derived from the WAX9 protein sequence
recognized a band of approximately 10 kDa in Western blots of crude cryoprotectin preparations.
Cryoprotective activity could be precipitated from solution by the antiserum. To clarify the function of the
different members of the gene family the five wax genes so far known are cloned and expressed in E. coli.
Wax b expressed in E. coli had lipid transfer activity but no cryoprotective activity. Wax e isolated from
cabbage cuticula also had lipid transfer activity but no cryoprotective activity. In contrast highly purified
fractions of cryoprotectin showed no lipid transfer activity but strong cryoprotective activity. Work is in
progress to clone further genes with the aim to identify the cryoprotective member of this gene family.


presented at: 6TH INTERNATIONAL PLANT COLD HARDINESS SEMINAR 30.6. - 5.7.2001, Helsinki, Finland